Download OU M.Pharma Ph.Analysis 2nd Sem 2018 1205PCI Advance Instrumental Analysis Question Paper

Download OU (Osmania University) M.Pharma-Ph.Analysis (Master of Pharmacy) 2nd Semester 2018 1205PCI Advance Instrumental Analysis Previous Question Paper

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Code No. 1205/PCI
FACULTY OF PHARMACY
M. Pharmacy (Pharm. Analysis) II-Semester (PCI) (Main) Examination,
August 2018
Subject: Advance Instrumental Analysis
Time: 3 Hrs Max. Marks: 75
Note: Answer any five questions. All questions carry equal marks.
1 a. Explain abt varis types of column s and column problems in HPLC. (9)
b. Write the principle and advantages of Ultra and Nano liquid chromatography? (6)
2 a. Discuss abt ion exchange chromatography and write in detail abt its
applications? (7)
b. Explain the varis components of HPTLC and write its advantages over
column chromatography? (8)
3 a. Write abt varis detectors used in GLC? (10)
b. Explain the principle and basic configuration of capillary electrophoresis? (5)
4 Elaborate with neat sketch, the instrumentation of mass spectrometry? (15)
5 a. What do y mean by chemical shift? Explain the varis factors influencing
it? (10)
b. Explain abt nuclear dble resonance and its applications? (5)
6 a. Mention varis tandem MS/MS systems and explain any one briefly with neat
sketch? (9)
b. Discuss the principle and applications of size exclusion chromatography? (6)
7 a. Explain abt preparative HPLC? (7)
b. Discuss abt FT NMR with reference to C
13
NMR (8)
8 a. Explain abt LC -NMR hyphenation. (9)
b. Write abt fragmentation ruleS in MS? (6)
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