Download OU M.Pharma Ph.Analysis 2nd Sem 2020 6134PCI Advance Instrumental Analysis Question Paper

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Code No. 6134/PCI

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FACULTY OF PHARMACY

M. Pharmacy (Pharma. Analysis) II-Semester (PCI) (Suppl.) Examination, January 2020

Subject : Advance Instrumental Analysis

Time: 3 Hrs Max. Marks: 75

Note: Answer Any Five Questions. All Questions Carry Equal Marks.

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1. a) Explain about various parameters like peak shape, capacity factor, plate number, plate height and resolutions to be considered in HPLC chromatogram. (10)
   b) Write about HPLC importance in chiral analysis of pharmaceuticals? (5)
2. a) Discuss about ion pair chromatography. (5)
   b) Explain the instrumentation and pharmaceutical applications of HPTLC. (10)
3. a) Write the principle and instrumentation of SFC? (7)
   

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   b) Explain about CE -MS Hyphenation? (8)
4. a) Elaborate with neat sketch diagram different types of ionization techniques and analyzers in mass spectrometry? (15)
5. a) What do you mean by chemical shift? Explain the various factors influencing it? (10)
   b) Write about correlative spectroscopy? (COSY) (5)
6. a) Write about various columns used in GLC? (8)
   

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   b) Discuss the principle and applications of size exclusion chromatography? (7)
7. a) Explain about HILIC approach in HPLC? (7)
   b) Discuss about ¹³C NMR (8)
8. a) Explain about Q -TOF hyphenation (MS.MS) (7)
   b) Write the principle and stationary phases used in affinity chromatography? (8)

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