Download OU (Osmania University) M.Pharma-Ph.Analysis (Master of Pharmacy) 2nd Semester 2019 13179PCI Advance Instrumental Analysis Previous Question Paper
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Code No. 13179/PCI
FACULTY OF PHARMACY
M. Pharmacy (Pharmaceutical Analysis) II-Semester (PCI) (Suppl.) Examination,
February 2019
Subject: Advance Instrumental Analysis
Time: 3 Hrs Max. Marks: 75
Note: Answer any five questions. All questions carry equal marks.
1 Write the principle involved in HPLC and explain the following.
(a) Peak shapes (b) Plate number (c) Plate height (10)
(d) Explain varis pumps used in HPLC. (5)
2 Explain the principle and stationary phases of the following: (2x7?)
(a) Ion Exchange chromatography (b) Affinity chromatography
3 Write in detail abt Instrumentation, columns and detectors used in Gas
chromatography. (15)
4 (a) Explain the instrumentation and applications of super critical fluid
chromatography. (7)
(b) Explain characteristics and pharmaceutical analysis of capillary
electrophoresis. (8)
5 (a) Explain the following ionization techniques
(a) chemical ionization (b) FAB (c) ESI (9)
(b) Explain fragmentation pattern of
(a) Alcohols (b) Aldehydes (c) aliphatic acids (6)
6 Explain the following: (3x5)
(a) Spin-spin cpling
(b) Cpling constant
(c) Nuclear magnetic dble resonance
7 Write abt the principles ins trumentation and applications of : (2x7?)
(a) TLC
(b) Size exclusion chromatography
8 (a) Explain in detail abt chiral stationary phases (CSP?s). (6)
(b) Explain principle and applications of HPTLC. (9)
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This post was last modified on 19 July 2020