Download OU M.Pharma Ph.Chemistry 2nd Sem 2019 13323PCI Advanced Spectral Analysis Question Paper

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Code No. 13323/PCI

FACULTY OF PHARMACY

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M. Pharmacy (Pharmaceutical Chemistry) II-Semester (PCI) (Main) Examination, August 2019

Subject: Advanced Spectral Analysis

Time: 3 Hrs Max. Marks: 75

Note: Answer any five questions. All questions carry equal marks.

1. (a) Discuss Woodward Fieser rule with examples? Discuss the calculation of ? max for cyclic dienes and unsaturated carbonyl compounds with examples. (8+7)
   

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   (b) Discuss how IR spectra is useful in structural elucidation of organic compounds with any four structures. (8+7)
2. Write a detailed account on:
   (a) 1-D NMR
   (b) INADEQUATE
3. (a) Discuss Mc Lafferty rearrangement and Ring rule.
   

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   (b) Give the mass fragmentation rule for amine, carbonyl compounds and halides. (7+8)
4. Explain the Principle, instrumentation and applications of following:
   (a) HPTLC (b) GC-MS (8+7)
5. Give the instrumentation and applications of following: (8+7)
   (a) DTA (b) DSC

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6. Write a short note on: (8+7)
   (a) HPTLC
   (b) Super critical fluid chromatography
7. Explain the Principle and applications of following: (8+7)
   (a) COSY (b) HECTOR

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8. Write a short note on: (8+7)
   (a) ELISA
   (b) Bio assay of digitalis