Rajiv Gandhi University of Health Sciences
First Year M.Pharm Degree Examination – May 2011
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[Time: 3 Hours] [Max. Marks: 100]
ADVANCED PHARMACEUTICAL ANALYSIS
PAPER IV
(RS 2 & RS 3)
Q.P. CODE: 9294
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Your answers should be specific to the questions asked.
Draw neat labeled diagrams wherever necessary. Answer all questions
LONG ESSAY (Answer any TWO) 2 X 20 = 40 Marks
- What are pyrogen? Explain its properties and methods of testing as mentioned in pharmacopoeia
- Explain two methods each for determination of heavy metal and pesticide residue in herbal preparations
- Explain the methodology and interpretation of cup plate method of antibiotic assay
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SHORT ESSAY (Answer any FIVE) 5 X 10 = 50 Marks
- Explain the principle and procedure of diphtheria antitoxin assay
- Write a note on test for endotoxin
- How is HPLC method validated
- Compare and contrast instrumental and volumetric methods of analysis
- Explain the principle involved in differential thermal analysis of a compound with relevant equations and graphs
- Classify chromatography. Explain qualitative application of planar chromatography
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SHORT NOTES 2 X 5 = 10 Marks
- Explain the principles of estimation of sulphanilamide by bratton - marshall reagent
- What are the applications of Radio - immuno assay
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