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Code No. 4264
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FACULTY OF PHARMACY
Pharm. D (6 YDC) lll-Year (Main) Examination, July 2017
Subject : Pharmaceutical Analysis
Time : 3 Hrs Max. Marks: 70
Note: Answer all questions from Part - A and answer any five questions from Part-B.
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PART - A (10 x 2 = 20 Marks)
- Write the principle involved in gel filtration.
- Define linearity and robustness.
- Name different type of detectors use in GLC.
- Distinguish between HPLC and HPTLC.
- Define Hook’s law and write its equation.
- Write abt the reference electrode used in potentiometry.
- Explain the principle of separation involved in ion exchange chromatography
- Write the composition of karlfischer reagent.
- Explain different ions in mass spectroscopy.
- Write the principle involved in AAS.
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PART - B (5 x 10 = 50 Marks)
- Write short note on :
- ICH - guidelines
- Regulatory control
- Discuss the principle and instrumentation of IR spectroscopy.
- Explain the principle and instrumentation of gel electrophoresis.
- Discuss the principle and different amperometric titration.
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- Write abt different analyzers used in Mass spectroscopy.
- Define chemical shift and list the varis factors affecting it.
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- Write the instrumentation and applications of HPTLC.
- Explain the principle and development technique of column chromatography.
- Describe the construction and working of X-Ray diffraction methods.
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