Download OU Pharm D Question Paper 3rd Sem 2017 4264 Pharmaceutical Analysis

FirstRanker.com

Code No. 4264

FACULTY OF PHARMACY

--- Content provided by‌ FirstRanker.com ---

Pharm. D (6 YDC) lll-Year (Main) Examination, July 2017

Subject : Pharmaceutical Analysis

Time : 3 Hrs Max. Marks: 70

Note: Answer all questions from Part - A and answer any five questions from Part-B.

PART - A (10 x 2 = 20 Marks)

--- Content provided by‌ FirstRanker.com ---

1. Write the principle involved in gel filtration.
2. Define linearity and robustness.
3. Name different type of detectors use in GLC.
4. Distinguish between HPLC and HPTLC.
5. Define Hook’s law and write its equation.

--- Content provided by‌ FirstRanker.com ---

6. Write about the reference electrode used in potentiometry.
7. Explain the principle of separation involved in ion exchange chromatography
8. Write the composition of Karl Fischer reagent.
9. Explain different ions in mass spectroscopy.
10. Write the principle involved in AAS.

--- Content provided by FirstRanker.com ---

PART - B (5 x 10 = 50 Marks)

11. Write short note on :
    • (a) ICH - guidelines
    • (b) Regulatory control
12. Discuss the principle and instrumentation of IR spectroscopy.

--- Content provided by FirstRanker.com ---

13. Explain the principle and instrumentation of gel electrophoresis.
14. Discuss the principle and different amperometric titration.
15. (a) Write about different analyzers used in Mass spectroscopy.
    (b) Define chemical shift and list the various factors affecting it.
16. Write the instrumentation and applications of HPTLC.

--- Content provided by​ FirstRanker.com ---

17. Explain the principle and development technique of column chromatography.
18. Describe the construction and working of X-Ray diffraction methods.