Code No. 1114
FACULTY OF PHARMACY
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Pharm. D (6 YDC) lll - Year (Instant) Examination, March 2018
Subject: Pharmaceutical Analysis
Time : 3 Hrs Max. Marks: 70
Note: Answer all questions from Part - A and answer any five questions from Part-B.
PART - A (10 x 2 = 20 Marks)
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- What are the advantages of HPTLC over HPLC?
- Write a note on spraying reagents used in Paper Chromatography.
- Write and explain Ilkovic equation.
- Write the sources of IR Spectroscopy.
- Define Quenching and Chromophore.
- Write the principle involved in Ion Exchange Chromatography
- Write a note on Karl Fischer Titration.
- Classify Chromatography based on its separation technique.
- Write a note on Preparative TLC.
- Write a note on solvent effects on UV spectroscopy.
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PART - B (5 x 10 = 50 Marks)
- Write a note on Total Quality Management.
- Write the principle, Instrumentation and Applications of Fluorimetry
- Write a note on Gel Electrophoresis.
- Write short notes on:
- Columns used in HPLC
- Detectors used in GLC
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- Write a note on Principle, Construction and Applications of Amperometric Titrations.
- Write the principle and Instrumentation of Mass Spectroscopy.
- Discuss the applications of the following in Pharmaceutical Analysis:
- Thermal Analysis
- X-Ray Diffraction
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- Discuss the Principle, Instrumentation and Applications of UV-Visible Spectroscopy.
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