Download GTU B.Pharma 2018 Winter 6th Sem 2260003 Pharmaceutical Analysis Iv Question Paper

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GUJARAT TECHNOLOGICAL UNIVERSITY
B.PHARM - SEMESTER - 6- EXAMINATION -WINTER - 2018
Subject Code:2260003 Date: 20/11/2018
Subject Name: Pharmaceutical Analysis IV
Time:02:30 PM TO 05:30 PM Total Marks: 80

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Instructions:

1. Attempt any five questions.
2. Make Suitable assumptions wherever necessary.
3. Figures to the right indicate full marks.

1. (a) What are x-rays? How they can be generated? Derive Bragg's equation and enlist the applications of x-ray diffraction. 06

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2. (b) Define and explain Radio Immuno Assay in detail. 05
3. (c) Write a short note on Nephelometry and Turbidimetry. 05

1. (a) Define validation. Enlist validation parameters and explain each in brief. 06
2. (b) What is IPR? Give some account on steps for filling patent. 05
3. (c) Write a short note on Raman Spectroscopy. 05

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1. (a) Explain basic principle, theory and applications of ion exchange and size exclusion chromatography. 06
2. (b) Enlist the similarities and differences between HPLC & HPTLC. 05
3. (c) Write a short note on ELISA. 05

1. (a) Discuss theory and principle of GC. Draw the instrumental diagram and explain the detectors used for GC. 06
2. (b) Explain basic principle, theory and applications of Super Critical Fluid Chromatography. 05

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3. (c) Write a short note on ISQ 9001:2000. 05

1. (a) Define radioactive compound. Explain isotopes dilution analysis and liquid scintillation system. 06
2. (b) Discuss in brief GATT and TRIPS. 05
3. (c) Write a short note on GLP. 05

1. (a) Explain the theory and principle of HPLC. Discuss in detail the instrumentation of HPLC with diagram. 06

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2. (b) Discuss different mobile and stationary phases for GC. 05
3. (c) Enlist the applications of partition and adsorption chromatography. 05

1. (a) Write a short note on mobile and stationary phases for normal and reversed phase HPLC. Enlist the applications of HPLC. 06
2. (b) Give the overview of LC-MS and LC-MS/MS. 05
3. (c) Explain the interaction of nuclear radiation with matter. What are the units of radio activity? How radio activity can be measured? 05

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