OCTOBER 2019 Sub. Code: 3814
PHARM. D DEGREE EXAMINATION
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(2009-2010 Regulation)
THIRD YEAR
PAPER II - PHARMACEUTICAL ANALYSIS
Q.P. Code: 383814
Time : Three hours Maximum : 70 Marks
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- Elaborate on: (4 x 10 =40)
- Explain the construction and working principle of Spectro fluorimeter.
- Give an account of theory and applications of X-ray diffraction technique.
- Explain in detail about ion exchange chromatography.
- What is thermal analysis? Explain the principle and instrumentation of DSC.
- Write notes on: (6x5=30)
- Write briefly on chemical shift in NMR.
- What are all the validation parameters performed during method development?
- Write the interference produced in flame photometer. How will you overcome this problem?
- What are the factors affecting electrical conductivity in solution?
- Describe the various types of vibration in IR.
- Write the reason for deviation of Beer’s law.
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