Download PTU M-Pharma 2019 May 2nd Semester 74925 ADVANCED INSTRUMENTAL ANALYSIS Question Paper

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Total No. of Pages : 01

Total No. of Questions : 06

M.Pharmacy(Pharmaceutical Analysis) (2017 Batch) (Sem.-2)

ADVANCED INSTRUMENTAL ANALYSIS

Subject Code : MPA-201T

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M.Code : 74925

Time: 3 Hrs.

Max. Marks : 75

INSTRUCTIONS TO CANDIDATES :

1. Attempt any FIVE questions out of SIX questions.

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2. Each question carries FIFTEEN marks.

Q1. Write a note on :

1. Ion exchange chromatography. (5)
2. HPLC in chiral analysis of pharmaceuticals. (5)
3. Capillary Electrophoresis. (5)

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Q2. A. Discuss principle, instrumentation and solvent requirement in NMR. (8)

B. Discuss briefly about FAB and chemical ionization mass spectrometry. (7)

Q3. A. Write about general principles of affinity chromatography. Write a note on stationary and mobile phases used in affinity Chromatography. (8)

B. Write a note on detectors used in HPLC. (7)

Q4. A. Elaborate on different mass analyzers. (8)

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B. Write briefly about principle of FT-NMR with reference to ¹³C-NMR. (7)

Q5. Write a note on :

1. Coupling constant. (5)
2. Matrix Assisted Laser Desorption (MALDI) (5)
3. Applications of NMR spectroscopy. (5)

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Q6. A. Write a note on CE-MS hypenation. (8)

B. Discuss principle and application of super critical fluid chromatography. (7)

NOTE : Disclosure of Identity by writing Mobile No. or Making of passing request on any page of Answer Sheet will lead to UMC against the Student.

(S31)-349

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