Rajiv Gandhi University of Health Sciences

First Year M. Pharm Degree Examination - JAN-2019

[Time: 3 Hours] [Max. Marks: 100]

MODERN PHARMACEUTICAL ANALYSIS

(OS & RS)

Q.P. CODE: 7891

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Your answers should be specific to the questions asked.

Draw neat labeled diagrams wherever necessary. Answer FOUR questions

ANSWER ANY FOUR 4 X 25 = 100 Marks

1. 1. Give an account of the principle, instrumentation and applications of UV spectroscopy
   2. Add a note on Woodward’s rules.

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2. Write briefly on:
   1. ORD
   2. FT-IR
   3. Reversed phase TLC
   4. Student’s t-test.

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3. What do you know of:
   1. Spin —spin coupling
   2. Spin-spin and spin-Lattice relaxation
   3. 2D NMR
   4. ¹³C NMR

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4. What is chemical ionization mass spectrometry? Discuss the instrumentation and applications of this technique in pharmaceutical analysis. What is FABMS?
5. Give an account of:
   1. Electrophoresis
   2. RP-HPLC
   3. Circular dichroism

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   4. Literature sources
6. Write short notes on:
   1. GLC
   2. HPTLC

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