This download link is referred from the post: RGUHS M.Pharm 2nd Year Last 10 Years 2011-2021 Question Papers || Rajiv Gandhi University of Health Sciences
Second Semester M.Pharm Degree Examination - FirstRanker.com
[Time: 3 Hours] [Max. Marks: 75]
Advanced Instrumental Analysis
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Q.P. CODE: 5149
Your answers should be specific to the questions asked.
Draw neat, labeled diagrams wherever necessary.
LONG ESSAY (Answer any Three) 3 X 10 = 30 Marks
- Describe the principle and instrumentation of ATR-IR.
- Explain the fragmentation patterns for alcohols and carbonyl compounds.
- Discuss the NOESY and COSY techniques of NMR spectroscopy.
- Write the principle, instrumentation and applications of ICP-MS.
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SHORT ESSAY (Answer any Nine) 9 X 5 = 45 Marks
- Write the principle and applications of RIA.
- Discuss the Woodward - Fieser rule for α, β-carbonyl compounds.
- Write the principle and applications of super critical fluid chromatography.
- Explain the concept of cotton effect in ORD.
- Discuss the principle and instrumentation of TGA.
- Give the IR absorption frequencies and NMR peaks for the following compounds i) Ethyl methyl ketone ii) Benzamide
- Explain Ring rule and isotope peak with suitable examples.
- Write a note on circular dichroism.
- Discuss the principle and applications of HPTLC.
- Identify the structure of an organic molecule consistent with the following spectra data
- Molecular formula : C4H8O2
- IR bands (cm-1) : 2981, 1752, 1390, 1250, 1055
- NMR peaks (δ) : 1.3 (triplet 3H), 2.1 (singlet 3H), 4.0 (quartet 2H)
- Mass spectra peaks : 88, 61, 45, 43
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This download link is referred from the post: RGUHS M.Pharm 2nd Year Last 10 Years 2011-2021 Question Papers || Rajiv Gandhi University of Health Sciences