Rajiv Gandhi University of Health Sciences
Second Semester M. Pharmacy Examination
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[Time: 3 Hours] [Max. Marks: 75]
Advanced Spectral Analysis-III
Q.P. CODE: 5157
Your answers should be specific to the questions asked.
Draw neat, labeled diagrams wherever necessary.
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LONG ESSAY (Answer any Three) 3 X 10 = 30 Marks
- Explain the instrumentation and applications of ATR-IR.
- Outline the theory and applications of 2D NMR.
- Explain the fragmentation of important functional group.
- Write the principle, instrumentation and applications of GC-AAS.
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SHORT ESSAY (Answer any Nine) 9 X 5 = 45 Marks
- Explain Woodward-Fieser rule for cyclic dienes.
- How will you identify the following functional groups in an organic compound (-OH, N-H, C-H, C-O, C=C) by IR-spectroscopy.
- Explain in detail Mc. Lafferty rearrangement.
- Give brief account on INADEQUATE techniques.
- Write the theory and applications of flash chromatography.
- Write the principle and applications involved in DSC.
- Give a brief account on Radio immuno assay of Insulin.
- Explain in brief interfacing CE with MS.
- Explain the principle and applications of Raman spectroscopy.
- Explain in brief biological standardization.
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