RGUHS M.Pharm 2nd Year Last 10 Years 2011-2021 Question Papers || Rajiv Gandhi University of Health Sciences
Second Semester M. Pharm Degree Examination
[Time: 3 Hours] [Max. Marks: 75]
Advanced Instrumental Analysis - II
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Q.P. CODE: 5149
Your answers should be specific to the questions asked.
Draw neat, labeled diagrams wherever necessary.
LONG ESSAY (Answer any Three) 3 X 10 = 30 Marks
- Define Mass Fragmentation. Explain all the Fragmentation rules with examples.
- Define EC-MS. Discuss principle instrumentation and applications of EC-MS.
- What are the advantages of 2-D NMR over 1-D NMR? Short note on NOESY and HECTOR.
- Describe ATR-IR technique and Wood-Ward Fieser rule for butadienes.
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SHORT ESSAY (Answer any Nine) 9 X 5 = 45 Marks
- Explain how TGA is used in qualitative and quantitative determinations.
- Explain in detail ring rule and isotopic peaks.
- Explain in detail about high-performance thin layer chromatography.
- Give the interpretation of any five organic functional groups by IR spectroscopy.
- Determination of rotation of optical activity by octant rule in ORD.
- Add a note on meta stable and isotopic peaks in MS.
- Discuss the RIA techniques.
- Add a note on Flash Chromatography.
- Discuss in detail LC-MS interface.
- Describe the importance and applications of DSC.
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