Rajiv Gandhi University of Health Sciences
First Year M.Pharm Degree Examination — Oct/Nov 2014
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[Time: 3 Hours] [Max. Marks: 100]
ADVANCED PHARMACEUTICAL ANALYSIS
PAPER IV
(RS 2 & RS 3)
Q.P. CODE: 9294
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Your answers should be specific to the questions asked.
Draw neat labeled diagrams wherever necessary. Answer all questions
LONG ESSAY (Answer any TWO) 2 X 20 = 40 Marks
- What do you mean by Thermal Analytical Method? Write a detailed note of differential Thermal Analysis (DTA). Add a note on applications of DTA in Pharmaceutical analysis and pre-formulation studies.
- What is a microbiological assay? Explain in Detail. Write a detailed note on microbiological assay of any antibiotic of your choice.
- Explain the principle and procedure involved in the biological assay of Gas Gangrene antitoxin.
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SHORT ESSAY (Answer any FIVE) 5 X 10 = 50 Marks
- Write a note on Radioimmunoassay (RIA).
- Write the principle and procedure involved in pyrogen testing as per I.P.
- Write a note on Validation parameters of HPLC Method.
- Write a brief note on drug quantification by mass spectrometry
- Write the principle and procedure involved in the biological assay of Oxytocin.
- Write a note on sterility testing.
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SHORT NOTES 2 X5 = 10 Marks
- Write a brief note on Thermo gravimetric Analysis.
- Explain briefly the biological assay of Urokinase.
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