Download RGUHS (Rajiv Gandhi University of Health Sciences) M.Pharma 2014 November (Master of Pharmacy) 1st Year 9359 Instrumental Method Of Analysis Revised Scheme 4 Previous Question Paper

Rajiv Gandhi University of Health Sciences, Karnataka
First Year M. Pharm Degree Examination ? Oct/Nov 2014
Time: Three Hours

Max. Marks: 100 Marks
INSTRUMENTAL METHOD OF ANALYSIS
(Revised Scheme 4)
Q.P. CODE: 9359
Your answers should be specific to the questions asked.
Draw neat labeled diagrams wherever necessary
LONG ESSAYS (Answer any Two)
2 x 20 = 40 Marks
1.
Explain detail principles and procedures involved in the methods of analysis for following
dosage forms.
a) Anti-tubercular drugs b) Local anaesthetics c) Sulphonamides
2.
Discuss principle and procedures involved in the quantitative determination of Carbonyl
group, carboxylic acid and amines.
3
a) Explain methods of particle size analysis and X-ray powder diffraction.
b) Discuss theory and applications of Raman Spectroscopy and Inductively Coupled Plasma-
Optical Emmision Spectrometers (ICP-OES).
SHORT ESSAYS (Answer any FIVE)
5 x 10 = 50 Marks
4.
Describe principle and procedure involved in the use of Ninhydrine & FC reagents in
pharmaceutical analysis.
5.
Write various quantitative methods of analysis of diuretics and analgesics & antipyretics.
6.
Write principle and procedures involved in the analysis of steroids and antibiotics.
7.
Write note on the following a) Turbidimetry b) Quality control of Radiopharmaceuticals.
8.
Describe application of instrumental methods in product characterization for product
development.
9.
Write a note on methods of analysis for sulphonamides.
SHORT NOTES
2 x 5 = 10 Marks
10.
Discuss application of SEM in particle size analysis.
11.
Write note on ICH guidelines in method validation.
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