Q.P. CODE: 7891
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Draw neat labeled diagrams wherever necessary. Answer FOUR questions
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ANSWER ANY FOUR 4 X 25 = 100 Marks
- a) Describe HPLC instrumentation with help of a block diagram.
b) Enumerate quantitative methods used in GC. - a) How do you do interpretation of IR-Spectra of organic compounds. Explain
b) Different sampling techniques used in IR – spectroscopy. - Write notes on
a) Circular dichroism
b) Moving Boundary Electrophoresis
c) HPTLC - a) Explain the principles and theoretical basis of PMR spectroscopy.
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b) What are
i) Chemical shift concept
ii) De - coupling and shift reagents
How they are useful in deciding the chemical structure. - a) What is fragmentation. Explain different fragmentation rules and patterns in Mass spectroscopy.
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b) Write about Fast atom bombardment Ionization technique. - a) Write Woodward's rules for calculating absorption maximum of carbonyl Compounds.
Multicomponent analysis by UV – Spectrophotometry.
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