Download OU M.Pharma Pharmaceutics 1st Sem 2019 13303PCI Modern Pharmaceutical Analytical Techniques Question Paper

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Code No. 13303/PClI

FACULTY OF PHARMACY

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M. Pharmacy (Common paper for all Specialization) I-Semester (PCI) (Suppl.)

Examination, August 2019

Subject : Modern Pharmaceutical Analytical Techniques

Time: 3 Hrs Max. Marks: 75

Note: Answer any five questions. All questions carry equal marks.

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1. 1. Write Beer-Lambert’s law and derive the expression 5
   2. Mention the different methods of quantitative analysis by uv-visible spectroscopy. Explain any one method in detail. 10
2. 1. Explain the interpretation procedure of IR spectra of different organic compnds in detail. With examples of schematic IR spectra.
   2. What is fluorescence? Write the factors affecting fluorescence. 5

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3. 1. What is chemical shift? Write the factors influencing chemical shift? 8
   2. Write a note on FT-NMR 7
4. 1. Explain the instrumentations and working of mass spectrometer with schematic diagram. 8

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   2. Write the fragmentation patterns of different organic compnds observed in mass spectroscopy. With the help of schematic mass spectra of a few compnds 7
5. Describe the components and working procedure of HPLC with a neat labeled block diagram. 15
6. 1. Write the principle, instrumentation and working of zone electrophoresis. 8
   2. Write the principle and theory of X-ray diffraction study using Brag’s law 7

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7. 1. Write the principle and instrumentation of flame photometry 7
   2. Write notes on any two GC detectors 8
8. Explain the principle, equipment, procedure, advantages and applications of IR Spectrophotometer 15

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