Download OU M.Pharma Ph.Chemistry 2nd Sem 2019 13323PCI Advanced Spectral Analysis Question Paper

Download OU (Osmania University) M.Pharma-Ph.Chemistry (Master of Pharmacy) 2nd Semester 2019 13323PCI Advanced Spectral Analysis Previous Question Paper

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Code No. 13323/PCI
FACULTY OF PHARMACY
M. Pharmacy (Pharmaceutical Chemistry) II-Semester (PCI) (Main) Examination,
August 2019
Subject: Advanced Spectral Analysis
Time: 3 Hrs Max. Marks: 75
Note: Answer any five questions. All questions carry equal marks.
1 (a) Discuss Woodward Fieser rule with examples ? Discuss the calculation of ? max
for cyclic dienes and unsaturated carbonyl compnds with examples . (8+7)
(b) Discuss how IR spectra is useful in structural elucidation of organic
compnds with any fr structures .
2 Write a detailed accnt on : (8+7)
(a) 1-D NMR
(b) INADEQUATE
3 (a) Discuss Mc Lafferty rearrangement and Ring rule.
(b) Give the mass fragmentation rule for amine, carbonyl compnds and
halides. (7+8)
4 Explain the Principle, instrumentation and applications of following
(a) HPTLC (b) GC-MS (8+7)
5 Give the instrumentation and applications of following : (8+7)
(a) DTA (b) DSC
6 Write a short note on : (8+7)
(a) HPTLC
(b) Super critical fluid chromatography
7 Explain the Principle and applications of following : (8+7)
(a) COSY (b) HECTOR
8 Write a short note on : (8+7)
(a) ELISA
(b) Bio assay of digitalis
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