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Rajiv Gandhi University of Health Sciences, Karnataka
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First Year M. Pharm Degree Examination – May 2016
Time: Three Hours
Max. Marks: 100 Marks
INSTRUMENTAL METHOD OF ANALYSIS
(Revised Scheme 4)
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Q.P. CODE: 9359
Your answers should be specific to the questions asked.
Draw neat labeled diagrams wherever necessary
LONG ESSAYS (Answer any Two)
2 x 20 = 40 Marks
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a) Describe various methods employed in the particle size analysis. (10+10)
b) Discuss the principle and applications of Raman spectroscopy.
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Discuss the principle involved in the analysis of two barbiturates and two anti-tubercular drug. (20)
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a) Principle involved in the assay of Vitamin A and Vitamin B2. (10+10)
b) Principle involved in quantitative estimation of drugs containing Carbonyl functional group and their applications.
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SHORT ESSAYS (Answer any FIVE)
5 x 10 = 50 Marks
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Describe the principle and procedure involved in analysis of any three alkaloids.
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Write briefly about different methods for the estimation of primary, secondary and tertiary amines.
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Mention the principle involved and applications of MBTH reagent and Bratton Marshall reagent.
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Describe the meaning of the following as per Pharmacopoeia.
- Expression of concentration
- Excipients
- Crude drug
- Storage
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Describe the analytical importance of 2,6-dichloroquinonechlorimide and Ninhydrin reagent.
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Write a brief note on instrumental methods for product characterization with examples.
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SHORT NOTES
2 x 5 = 10 Marks
- Validation of analytical methods.
- Principle involved in the analysis of radiopharmaceuticals.
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