Download RGUHS M.Pharmacy First Year 2014 November 9359 Instrumental Method Of Analysis Question Paper

Rajiv Gandhi University of Health Sciences, Karnataka

First Year M. Pharm Degree Examination – Oct/Nov 2014

Time: Three Hours

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Max. Marks: 100 Marks

INSTRUMENTAL METHOD OF ANALYSIS

(Revised Scheme 4)

Q.P. CODE: 9359

Your answers should be specific to the questions asked.

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Draw neat labeled diagrams wherever necessary

LONG ESSAYS (Answer any Two) 2 x 20 = 40 Marks

1. Explain detail principles and procedures involved in the methods of analysis for following dosage forms.
   1. Anti-tubercular drugs
   2. Local anaesthetics
   3. Sulphonamides

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2. Discuss principle and procedures involved in the quantitative determination of Carbonyl group, carboxylic acid and amines.
3. 1. Explain methods of particle size analysis and X-ray powder diffraction.
   2. Discuss theory and applications of Raman Spectroscopy and Inductively Coupled Plasma- Optical Emmision Spectrometers (ICP-OES).

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SHORT ESSAYS (Answer any FIVE) 5 x 10 = 50 Marks

4. Describe principle and procedure involved in the use of Ninhydrine & FC reagents in pharmaceutical analysis.
5. Write various quantitative methods of analysis of diuretics and analgesics & antipyretics.
6. Write principle and procedures involved in the analysis of steroids and antibiotics.
7. Write note on the following
   1. Turbidimetry

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   2. Quality control of Radiopharmaceuticals.
8. Describe application of instrumental methods in product characterization for product development.
9. Write a note on methods of analysis for sulphonamides.

SHORT NOTES 2 x 5 = 10 Marks

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10. Discuss application of SEM in particle size analysis.
11. Write note on ICH guidelines in method validation.

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