Rajiv Gandhi University of Health Sciences
First Year M. Pharm Degree Examination - NOVEMBER 2015
[Time: 3 Hours] [Max. Marks: 100]
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Modern Pharmaceutical Analysis (Revised Scheme 4)
Q.P. CODE: 9336
Your answers should be specific to the questions asked.
Draw neat, labeled diagrams wherever necessary.
LONG ESSAY (Answer any TWO) 2 X 20 = 40 Marks
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- Briefly outline the instrumentation of Mass Spectrometer. Discuss in detail about interpretation of organic functional groups by IR Spectroscopy. (10+10)
- Explain the functions of the various parts of an HPLC System. Discuss about selection of liquid stationary phases in GC. (12+8)
- Explain the fundamental principles and instrumental arrangements of NMR. Write a detail note on Octant rule. (14+6)
SHORT ESSAY (Answer any FIVE) 5 X 10 = 50 Marks
- Write fragmentation process in Mass spectroscopy.
- Explain the techniques involved in Isotachophoresis. Write theoretical aspects of derivative spectroscopy.
- Write a note on coupling and decoupling methods and its significance in NMR spectroscopy.
- State and derive an equation for Bragg’s Law. Explain the concept of Miller indices.
- Discuss in detail about the HPTLC technique.
- Explain the significance of ’T’ test and chi-square test with suitable examples.
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SHORT NOTES 2 X 5 = 10 Marks
- Discuss about Human volunteer research – informed consent.
- Write about FTIR technique.
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