(LD 4270)
AUGUST 2013
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Sub. Code: 4270FOURTH YEAR B.PHARM. EXAM
PAPER IV ? MODERN METHODS OF PHARMACEUTICAL
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ANALYSIS
Q.P. Code: 564270
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Time: Three HoursMaximum: 100 marks
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I. Elaborate on:
(2X20=40)
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1. a. Write in details about the principle involved in spectroscopy
b. Write the principle, working principle and application of
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Nephelo turbidimetry
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2. a. Write the theory & Principle in IR Spectroscopyb. Write the principle and working principle of Gas chromatography
with a neat diagram
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II. Write notes on:
(8X5=40)
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1. Standard calomel electrode2. Rheodyne injector
3. Electron Capture detector
4. a. Diffraction grating b. Tranmission Grating
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5. a. M +1 peak b. M + 2 peak c. Base peak6. Principle involved in paper chromatography
7. Polarography
8. Counter current extraction
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III. Short Answers on:(10X2=20)
1. Nernst Equation
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2. Dipole moment
3. Partition co efficient
4. Static Quenching
5. What is deuterated solvents
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6. How will you measure cell constant in conductometry7. Rf, Rx, Rm
8. Principle of separation on GLC
9. Five Examples for non reducible ions.
10. Half wave potential
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