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Rajah Jandhi University of Health Sciences
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First Year M. Pharm Degree Examination - MAY 2016
[Time: 3 Hours]
Modern Pharmaceutical Analysis
(Revised Scheme 4)
Q.P. CODE: 9336
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Your answers should be specific to the questions asked.
Draw neat, labeled diagrams wherever necessary.
LONG ESSAY (Answer any TWO) 2 X 20 = 40 Marks
- Define and derive an equation for Bragg's law. Explain the general rule for fragmentation pattern in mass spectrometry. (8+12)
- Write a detailed note on interaction of UV-visible radiation with organic compounds. Explain the theory and factors affecting electrophoresis. (8+12)
- Define chemical shift. Outline with a neat sketch about NMR instrumentation. Explain about FT-NMR.
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SHORT ESSAY (Answer any FIVE) 5 X 10 = 50 Marks
- Write in detail about the instrumentation of HPTLC.
- Explain interpretation of any five organic functional group by IR.
- Write in detail about the detectors and derivatisation techniques in GC.
- Discuss the phenomena of Circular Dichroism. Write a brief note on differential scanning calorimetry.
- Explain efficiency parameters of HPLC. How they are calculated from a chromatogram?
- Discuss various ionization techniques used in mass spectroscopy.
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SHORT NOTES 2 X 5 = 10 Marks
- Note on Text citation and Bibliography writing
- Student T-test with relevant example
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*****
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