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9294_2009_1_S43.doc
Rajiv Gandhi University of Health Sciences
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First Year M.Pharm Degree Examination – October 2010
[Time: 3 Hours] [Max. Marks: 100]
ADVANCED PHARMACEUTICAL ANALYSIS
PAPER IV
(Revised Scheme 2)
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Q.P. CODE : 9294
Your answers should be specific to the questions asked.
Draw neat labeled diagrams wherever necessary. Answer all questions
LONG ESSAY (Answer any TWO) 2 X 20 = 40 Marks
- Explain in detail how residual pesticides can be quantitated by mass spectrometry
- Explain the principle & the methodology involved in the biological assay of
- Heparin sodium
- Rabies vaccine
- Explain the methodology & instrumentation involved in the differential scanning calorimetric analysis. Give its important applications in pharmacy
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SHORT ESSAY (Answer any FIVE) 5 X 10 = 50 Marks
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- Give the importance of radiopharmaceuticals with suitable examples
- Explain the pyrogen test I.P
- Explain clearly how a UV-VIS spectrophotometer can be validated
- Give the importance of standard deviation (SD) & relative standard deviation (RSD) you have studied
- Give the microbial assay of any
- Explain how oxytocin is assayed
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SHORT NOTES 2 X 5 = 10 Marks
- Parameters governing the performance of a UV-detector in HPLC
- Importance of slit-width in UV-spectrophotometer
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