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B. Pharm. - I Second Year (Annual Pattern) (New Course)
35010 : Pharmaceutical Analysis - I : IL.T.3
AW - 2265
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Max. Marks : 80
Notes: 1. All questions carry equal marks.
2. Answer any eight questions.
3. Diagrams and chemical equations should be given wherever necessary.
- Discuss about acid-base indicators. Write principle and procedure for assay of aspirin powder. (10)
- Discuss in detail about steps involved in gravimetric analysis. (10)
- Explain theory, scope, limitations of non-aqueous titration. (10)
- Write various types of complexometric titrations. Write assay procedure for calcium gluconate powder. (10)
- What are redox indicators? Explain the titration involving potassium permanganate. (10)
- Explain Volhard's method of precipitation titration. Write its advantages and disadvantages. (10)
- Explain about following terms- (10)
- Standard deviation
- Primary Standard
- Precision and accuracy
- What is diazotization? Explain principle of diazotization titration. (10)
- What is mean by complexation and chelation? Write a note on stability of complexes. (10)
- Write short note on any two. (10)
- Kjeldahl method of nitrogen estimation.
- Oxygen flask combustion method.
- Warner's co-ordination number.
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AW -2265
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