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Download Pharm D 3rd Year 2013 April 383814 Pharmaceutical Analysis Question Paper

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This post was last modified on 26 April 2022

Pharm D Last 12 Years 2010-2022 Question Papers (1st Year, 2nd Year, 3rd Year, 4th Year and 5th Year)


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[LC 814] APRIL 2013 Sub. Code: 3814

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DOCTOR OF PHARMACY (PHARM. D) DEGREE EXAMINATION

THIRD YEAR

PAPER II - PHARMACEUTICAL ANALYSIS

Q.P. Code: 383814

Time: Three Hours Maximum: 100 marks

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Answer All questions

  1. Elaborate on: (2x20=40)
    1. Explain the working and components of gas chromatograph with help of a neat, labeled, schematic block diagram. Write a note on classification, principle, factors influencing the separation and criteria to perform the Gas chromatography.
    2. a) Draw an UV-Visible double beam spectrophotometer with a neat, labeled, block diagram and explain its each component operational mode.
      b) Why a double beam spectrophotometer gives more precise, reliable and reproducible results in comparison to a single beam spectrophotometer?
      c) What are the factors influencing the absorption of radiant energy?
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  2. Write notes on: (10 x 6 =60)
    1. Give a brief and comprehensive account of application of conductometry?
    2. State Beer-Lambert’s law. Derive it Write its-application, deviation and limitation.
    3. Discuss the underlying principle and interference of atomic absorption spectrometry.
    4. Name the detectors used in HPLC. Discuss anyone of them.
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    6. Differentiate validation and calibration. Give a brief account of validation of analytical methods.
    7. Explain the theory and procedure of DSC.
    8. Discuss the fundamental theory of mass spectroscopy.
      What are the different ions produced in mass spectrum?
    9. What is quenching? What are different type of quenching?

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      Write a note on factors affecting the fluorescence intensity.
    10. Explain the various method of sample handling in IR-Spectroscopy.
    11. Give a brief account of :
      a) Indicator electrode, b) Polarizable electrode, c) Spectrophotometric titration.
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This download link is referred from the post: Pharm D Last 12 Years 2010-2022 Question Papers (1st Year, 2nd Year, 3rd Year, 4th Year and 5th Year)

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