Download Pharm D 3rd Year 2014 October Pharmaceutical Analysis Question Paper

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[LF 814]

OCTOBER 2014

Sub. Code: 3814



PHARM. D DEGREE EXAMINATION

(2009-2010 Regulation)

THIRD YEAR

PAPER II ? PHARMACEUTICAL ANALYSIS



Q.P. Code : 383814

Time : Three hours









Maximum : 70 marks


I. Elaborate on :



(4 x 10 = 40)



1. Explain the working principle and instrumentation of double beam UV-Vis

spectrophotometer with a neat diagram.

2. Describe the principle, various stationary and mobile phases used, development

and detection techniques of TLC.

3. What is electrophoresis? Explain the principle, instrumentation and applications

of gel electrophoresis.

4. Explain the principle and various types of interferences that are encountered

while performing analysis with flame emission spectroscopy.



II. Write notes on :

(6 x 5 = 30)



1. Elaborate on the theory of fluorescence. Explain how it can be used for

quantification of pharmaceutical compounds.



2. Explain the various sources and detectors used in IR spectroscopy.

3. Write a note on the theoretical aspects of NMR and ES

4. Explain the principle and instrumentation of polarimete

5. Write a note on DME and Ilkovic equation.

6. Define Rf value, retention time, HETP, Bathochromic shift and quenching.





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